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室温轧制对Nb3(Al0.96Ge0.04)缺陷的调控及性能的研究
  • ISSN:3041-0673(Print)3041-0681(Online)
  • DOI:10.69979/3041-0673.26.07.006
  • 出版频率:月刊
  • 语言:中文
  • 收录数据库:ISSN:https://portal.issn.org/ ;中国知网:https://scholar.cnki.net/journal/search ;RCCSE权威核心学术期刊:http://qk.nseac.com

室温轧制对Nb3(Al0.96Ge0.04)缺陷的调控及性能的研究
李文龙

西南交通大学物理科学与技术学院,四川省成都市,610031;

摘要:本文采用粉末装管法(PIT)制备了Nb3(Al0.96Ge0.04)前驱体圆线材并室温轧制成不同厚度的扁线材,通过减小线材尺寸来改变热处理过程中的传热条件。RHQ后,在Nb3(Al0.96Ge0.04)圆线中同时存在Nb(Al,Ge)ss和A15相。当线材厚度降低时,热量能够更快地传导与释放,这使得Nb(Al,Ge)过饱和固溶体更容易被保留下来。轧制后厚度为0.55 mm薄扁线在RHQ后,Nb3(Al0.96Ge0.04)得到了单一物相的Nb(Al,Ge)ss。在后续退火过程中,Nb(Al,Ge)ss向A15相转变时会产生大量可作为磁通钉扎中心的堆垛层错结构。厚度为1mm的Nb3(Al0.96Ge0.04)的扁线样品的临界电流密度相比于圆线提升了280%@4.2K,6T。通过厚度调控可促进Nb(Al,Ge)ss相的保留,退火后在样品中形成了更高密度的磁通钉扎中心。

关键词:Nb3(Al0.96Ge0.04);室温轧制;堆垛层错

参考文献

[1] Iijima Y, Kikuchi A, Inoue K. New Nb3Al-based A15 multifilamentary wires with high Jc in high fields[J]. Cryogenics, 2000, 40(4):4-5.

[2] Banno N,Uglietti D,Seeber B,et al. Strain dependence of superconducting characteristics in technical Nb3Al superconductors[J].Superconductor Science and Technology,2005,18(3):284.

[3] Hemmi T, Koizumi N, Nunoya Y, et al. Characterization of Nb3Al Strands Subjected to an Axial-Strain for a Fusion DEMO Reactor[J]. IEEE Transactions on Applied Superconductivity, 2009, 19(3):1540-1543.

[4] Takeuchi T. Nb3Al conductors for high-field applications [J]. Superconductor Science and Technology, 2000, 13(9): R101.

[5] Takeuchi T, Iijima Y, Inoue K, et al. Strain effects in Nb3Al multifilamentary conductors prepared by phase transformation from bcc supersaturated-solid solution [J]. Applied Physics Letters, 1997, 71(1): 122-124.

[6] Yamashita A, Matsuda T D, Mizuguchi Y. Synthesis of new high-entropy alloy-type Nb3(Al, Sn, Ge, Ga, Si) superconductors[J]. Journal of Alloys and Compounds, 2021, 868.

[7] Iijima Y, Kikuchi A, Inoue K, et al. Effects of additional elements to Nb3Al multifilamentary wire fabricated by Rapid-Heating/Quenching process[J]. IEEE Transactions on Applied Superconductivity, 1999, 9,(2):2696-2701.

[8] Kikuchi A, Iijima Y, Inoue K, et al. Fabrication of Nb3(Al, Ge) wires by using Al-Ge gas-atomized powder [J]. IEEE Transactions on Applied Superconductivity, 2003,13(2): 3446-3449.

[9] Pan X F, Yan G, Cui L J, et al. Fabrication and Superconducting Properties of Rod‐In‐Tube Multifilamentary Nb3Al Wire With Rapid Heating and Quenching Heat‐Treatment[J]. IEEE Transactions on Applied Superconductivity, 2014, 25(3): 1-4.

[10] Chen M, Chen X, Ran M, et al. Properties Comparison of RHQT Nb3(Al0.95Ge0.05) Superconductors Formed via Quenched bcc Phase With/Without Disordered A15 Present[J]. Journal of Superconductivity and Novel Magnetism, 2021, 34(7): 1893-1901.

[11] Yu Z, Xia L, Yang C K, et al. Phase Structure and Superconducting Properties of RHQT Nb3Al Wires Fabricated by Static and Dynamic Rapid Heating[J]. IEEE Transactions on Applied Superconductivity, 2020, 30(4): 1-5.

[13] 李国威. Ge、Sn共掺Nb3Al超导线材的制备及其性能[D]. 西南交通大学, 2022.

[14] 陈紫贤. 初中物理热学问题中热量的计算法与解题技巧[J] 数理化解题研究.

[15] Lombardi A, Sediako D, Machin A, et al. Effect of solution heat treatment on residual stress in Al alloy engine blocks using neutron diffraction[J]. Materials Science and Engineering: A, 2017, 697: 238-247.

[16] T'ing-Sui Ke. Viscous Slip Along Grain Boundaries and Diffusion of Zinc in Alpha‐Brass[J]. 1948, 19(3): 285-290.

[17] 陈筱莹. Ti,Ta掺杂Nb3Al线材的快热急冷转变成相过程和超导性能研究[D]. 西南交通大学, 2022.

[18] T'ing-Sui Ke. Viscous Slip Along Grain Boundaries and Diffusion of Zinc in Alpha‐Brass[J]. 1948, 19(3): 285-290.

[19] Changkun Y, Xiaguang S, Lian L, et al. Reproducible stable critical current density in powder-in-tube (PIT) Nb3Al superconductors by multi-time rapid heating and quenching process[J]. Intermetallics, 2023, 160: 107938.

[20] Togano K, Takeuchi T, Tachikawa K. A15-Nb3(Al,Ge) Superuperconductors Prepared by Transformation from Liquid Quenched Body-centered Cubic Phase[J]. Applied Physics Letters, 1982,41,(2):199-201.